| |
Multistep Organic Syntheses
- Chemical equipment and glassware to perform chemical reaction scales from 1mg to 100g.
- Solid phase syntheses.
- Temperature controlled reactions from -78oC to 200oC.
- High pressure Parr reactions to 5g, distillation, evaporation, and lyophilizations to 5L, sublimations to 1g.
- Photolysis reactions up to 3L.
Purifications
- Flash chromatography (silica gel, alumina, reverse phase).
- Size exclusion and ion exchange chromatography.
- Dialysis and gel filtrations.
- Prep HPLC (normal / reverse phase, ion exchange, size exclusion).
Analyses
- TLC
- DNA enzymatic digests.
- HPLC with PDA detection.
- UV-Vis Spectroscopy.
- Karl Fischer Titrations.
- Optical Polarimetery.
- Melting points.
- NMR (in conjunction with the Sealy Center for Structural Biology, or Dr. Scott Gilbertson’s NMR lab at UTMB).
- Mass Spectroscopy (through the UTMB Biomolecular Resource Core Facility).
|
